Publikationen

Publikationen

1 C. M. Thiele, S. Berger, Probing the Diastereotopicity of Methylene Protons in Strychnine Using Residual Dipolar Couplings, Org. Lett. 2003, 5, 705-708.
2 C. M. Thiele, T. N. Mitchell, Hydrostannylation of Propargylic Alcohols Using Mixed Tin Hydrides, Eur. J. Org. Chem. 2004, 337-353.
3 C. M. Thiele, T. N. Mitchell, Stille Coupling Reactions of functionalised triorganotin halides, Appl. Organomet. Chem. 2004, 83-85.
4 C. M. Thiele, Poly-γ-ethyl-Lglutamate as Alignment Medium for the Measurement of RDCs in Organic Substrates, J. Org. Chem. 2004, 69, 7403-7413.
5 C. M. Thiele, Book Review, Structure Elucidation by NMR in Organic Chemistry, A practical guide. 3rd revised edn. by E. Breitmaier, Magn. Res. Chem. 2004, 42, 368.
6 C. M. Thiele, Scaling the alignment of Polyglutamates by Variable Angle Sample Spinning, Angew. Chem. 2005, 117, 2847-2850, Angew. Chem. Int. Ed. 2005, 44, 2787-2790.
7 V. V. Klochkov, A. V. Klochkov, C. M. Thiele, S. Berger, A Novel Liquid Crystalline System for Partial Alignment of Organic Molecules, J. Magn. Res. 2006, 179, 58-63.
8 C. M. Thiele, Book Review, Essential NMR, B. Blümich, Macromol. Chem. Phys. 2006, 207, 910.
9 C. M. Thiele, A. Marx, R. Berger, J. Fischer, M. Biel, A. Giannis, Determination of the relative configuration of a five-membered ring compound using RDCs, Angew. Chem. 2006, 118, 4566-4571, Angew. Chem. Int. Ed. 2006, 45, 4455-4460.
10 C. M. Thiele, Use of RDCs in Rigid Organic Compounds and Some Practical Considerations concerning Alignment Media, Conc. Magn. Res. 2007, 30A, 65-80 (Review).
11 C. M. Thiele, Magnetic Resonance at or below the Earth's magnetic field, Angew. Chem. 2007, 119, 4904-4909; Angew. Chem. Int. Ed. 2007, 46, 4820-24.
12 C. M. Thiele, W. Bermel, J-modulated ADEQUATE experiments using different kinds of refocusing pulses, Magn. Res. Chem. 2007, 45, 889-894.
13 S. Leuthäußer, V. Schmidts, C. M. Thiele, H. Plenio, π-Face Donor Properties of N-Heterocyclic Carbenes in Grubbs II Complexes, Chem. Eur. J. 2008, 14, 5465-5481.
14 C. M. Thiele, Residual Dipolar Couplings (RDCs) in Organic Structure Determination, Eur. J. Org. Chem. 2008, 5673-5685.
15 A. Marx, C. M. Thiele, Orientational properties of PBLG: Influence of molecular weight and solvent on order parameters of the solute, Chem. Eur. J. 2009, 15, 254-260.
16 R. S. Stoll, M. V. Peters, A. Kühn, S. Heiles, R. Goddard, M. Bühl, C. M. Thiele, S. Hecht, Photoswitchable Catalysts: Correlating Structure and Conformational Dynamics with Reactivity by a Combined Experimental and Computational Approach, J. Am. Chem. Soc. 2009, 131, 357-367.
17 C. M. Thiele, K. Petzold, J. Schleucher, EASY ROESY: Reliable Cross-Peak Integration in Adiabatic Symmetrized ROESY, Chem. Eur. J. 2009, 15, 585-588.
18 A. Marx, V. Schmidts, C. M. Thiele, How different are diastereomorphous orientations of enantiomers in the liquid crystalline phases of PBLG and PBDG: a case study, Magn. Res. Chem. 2009, 47, 734-740.
19 C. M. Thiele, V. Schmidts, B. Böttcher, I. Louzao, R. Berger, A. Maliniak, B. Stevensson, On the Treatment of Conformational Flexibility when using Residual Dipolar Couplings for Structure Determination, Angew. Chem. 2009, 121, 6836-6840, Angew. Chem. Int. Ed. 2009, 48, 6708-6712.
20 C. M. Thiele, A. Maliniak, B. Stevensson, Use of Local Alignment Tensors for the Determination of Relative Configurations in Organic Compounds, J. Am. Chem. Soc. 2009, 131, 12878-12879.
21 B. Böttcher, V. Schmidts, J. A. Raskatov, C. M. Thiele, Determination of the Conformation of the Key Intermediate in an Enantioselective Palladium-Catalyzed Allylic Substitution from Residual Dipolar Couplings, Angew. Chem. 2010, 122, 210-214, Angew. Chem. Int. Ed. 2010, 49, 205-209.
22 A. Marx, B. Böttcher, C. M. Thiele, Enhancing the Orienting Properties of Poly(γ-benzyl-L-glutamate) by means of Additives, Chem. Eur. J. 2010, 16, 1656-1663.
23 L. Arnold, A. Marx, C. M. Thiele, M. Reggelin, Polyguanidines as Chiral Orienting Media for Organic Compounds, Chem. Eur. J. 2010, 16, 10342-10346.
24 U. M. Reinscheid, M. Köck, C. Cychon, V. Schmidts, C. M. Thiele, C. Griesinger, The Absolute Configuration of Dibromopalau'amine, Eur. J. Org. Chem. 2010, 6900-6903.
25 C. M. Thiele, W. C. Pomerantz, N. L. Abott, S. H. Gellman, Lyotropic liquid crystalline phases from helical &beta-peptides als alignment media, Chem. Commun. 2011, 47, 502-504 (Emerging Investigators Issue).
26 D. Zornik, R. M. Meudtner, T. El Malah, C. M. Thiele, S. Hecht, Designing Structural Motifs for Clickamers: Exploiting the 1,2,3-Triazole Moiety to Generate Conformationally Restricted Architectures, Chem. Eur. J. 2011, 17, 1473-1484.
27 G. Kummerlöwe, S. L. Grage, C. M. Thiele, I. Kuprov, A. S. Ulrich, B. Luy, Variable Angle NMR Spectroscopy and Its Application to the Measurement of Residual Chemical Shift Anisotropy, J. Magn. Reson. 2011, 209, 19-30.
28 C. M. Thiele, W. Bermel, Speeding up the measurement of one-bond scalar (1J) and residual dipolar couplings (1D) by using non-uniform sampling (NUS), J. Magn. Reson. 2012, 216, 134-143 / Corrigendum.
29 B. Böttcher, C. M. Thiele, Determining the Stereochemistry of Molecules from Residual Dipolar Couplings (RDCs), in Encyclopedia of Magnetic Resonance, (published by R. K. Harris, R. E. Wasylishen), John Wiley, Chichester, 2012.
30 R. Berger, J. Courtieu, R. R. Gil, C. Griesinger, M. Köck, P. Lesot, B. Luy, D. Merlet, A. Navarro-Vázquez, M. Reggelin, U. M. Reinscheid, C. M. Thiele, M. Zweckstetter, Is Enantiomer Assignment Possible by NMR Spectroscopy Using Residual Dipolar Couplings from Chiral Nonracemic Alignment Media? – A Critical Assessment, Angew. Chem. 2012, 124, 8512–8515, Angew. Chem. Int. Ed. 2012, 51, 8388–8391.
31 N.-C. Meyer, A. Krupp, V. Schmidts, C. M. Thiele, M. Reggelin, Polyacetylenes as Enantiodifferentiating Alignment Media, Angew. Chem. 2012, 124, 8459–8463, Angew. Chem. Int. Ed. 2012, 51, 8334–8338.
32 H.-G. Weinig, C. M. Thiele, 4. Chinesisch-Deutsches Symposium “Frontiers of Chemistry”, Nachr. Chem. 2012, 60, 1234-1235.
33 P. Giraudeau, T. Montag, B. Charrier, C. M. Thiele, Fast access to residual dipolar couplings by single-scan 2D NMR in oriented media, Magn. Reson. Chem. 2012, 50, S53–S57 / Corrigendum.
34 T. Montag, C. M. Thiele, Cross-Linked Helically Chiral Poly-(γ-benzyl-L-glutamate) as Enantiodiscriminating Alignment Medium, Chem. Eur. J. 2013, 19, 2271-2274.
35 V. Schmidts, M. Fredersdorf, T. Lübken, A. Porzel, N. Arnold, L. Wessjohann, C. M. Thiele, RDC-Based Determination of the Relative Configuration of the Fungicidal Cyclopentenone 4,6-Diacetylhygrophorone A12, J. Nat. Prod. 2013, 76, 839-844.
36 A. Kolmer, L. Kaltschnee, V. Schmidts, L. H. Peeck, H. Plenio, C. M. Thiele, The influence of electronic modifications on rotational barriers of bis-NHC-complexes as observed by dynamic NMR spectroscopy, Magn. Reson. Chem. 2013, 51, 695–700.
37 V. Thiel, K.-J. Wannowius, C. Wolff, C. M. Thiele, H. Plenio, Ring-Closing Metathesis Reactions: Interpretation of Conversion–Time Data, Chem. Eur. J. 2013, 19, 16403–16414.
38 I. Timári, L. Kaltschnee, A. Kolmer, R. W. Adams, M. Nilsson, C. M. Thiele, G. A. Morris, K. E. Kövér, Accurate determination of one-bond heteronuclear coupling constants with “pure shift” broadband proton-decoupled CLIP/CLAP-HSQC experiments, J. Magn. Reson. 2014, 239, 130-138.
39 L. Kaltschnee, A. Kolmer, I. Timári, V. Schmidts, R. W. Adams, M. Nilsson, K. E Kövér, G. A Morris, C. M. Thiele, „Perfecting“ pure shift HSQC: full homodecoupling for accurate and precise determination of heteronuclear couplings, Chem. Commun. 2014, 50, 15702-15705.
40 B. Horstmann, M. Korbus, T. Friedmann, C. Wolff, C. M. Thiele, F.-J. Meyer-Almes, Synthesis of azobenzenealkylmaleimide probes to photocontrol the enzyme activity of a bacterial histone deacetylase-like amidohydrolase, Bioorg. Chem. 2014, 57, 155-161.
41 K. Zhang, A. Geissler, M. Standhardt, S. Mehlhase, M. Gallei, L. Chen, C. M. Thiele, Moisture-responsive films of cellulose stearoyl esters showing reversible shape transitions, Sci. Rep. 2015, 5, 11011.
42 L.-G. Xie, V. Bagutski, D. Audisio, L. Wolf, V. Schmidts, K. Hofmann, C. Wirtz, W. Thiel, C. M. Thiele, N. Maulide, Dynamic Behaviour of monohaptoallylpaladium species: internal coordination as a driving force in allylic alkylation chemistry, Chem. Sci. 2015, 6, 5734-5739.
43 M. Fredersdorf, R. Göstl, A. Kolmer, V. Schmidts, P. Monecke, S. Hecht, C. M. Thiele, Exploring the Conformational Space of Bridge-Substituted Dithienylcyclopentenes, Chem. Eur. J. 2015, 21, 14545–14554.
44 J. Kind, C. M. Thiele, Still shimming or already measuring? – Quantitative reaction monitoring for small molecules on the sub minute timescale by NMR, J. Magn. Reson. 2015, 260, 109-115.
45 A. Kolmer, L. J. Edwards, I. Kuprov, C. M. Thiele, Conformational analysis of small organic molecules using NOE and RDC data: A discussion of strychnine and alpha-methylene-gamma-butyrolactone, J. Magn. Reson. 2015, 261, 101-109.
46 C. Wolff, J. Kind, H. Schenderlein, H. Bartling, C. Feldmeier, M. Biesalski, R. M. Gschwind, C. M. Thiele, Studies of a photochromic model system using NMR with ex-situ and in-situ irradiation devices, Magn. Reson. Chem. 2016, 54, 485-491.
47 N. Kolmer-Anderl, A. Kolmer, C. M. Thiele, M. Rehahn, Exploration of the photodegradation of naphto[2,3-g]quinoxalines and pyrazino[2,3-b]phenazines, Chem. Eur. J. 2016, 22, 5277–5287.
48 S. Hansmann, T. Larem (née Montag), C. M. Thiele, Enantiodifferentiating properties of the alignment media PELG and PBLG -- A comparison, Eur. J. Org. Chem. 2016, 7, 1324–1329.
49 F. Krohm, J. Kind, R. Savka, M. Alcaraz Janßen, D. Herold, H. Plenio, C. M. Thiele, A. Andrieu-Brunsen, Photochromic spiropyran- and spirooxazine-homopolymers in mesoporous thin films by surface initiated ROMP, J. Mater. Chem. C 2016, 4, 4067-4076 / Corrigendum.
50 C. M. Thiele, A. Kolmer, Response to “Comment on „Conformational Analysis of Small Organic Moleucles using NOE and RDC data: A discussion of strychnine and alpha-methylene-gamma-butyrolactone“” by I. A. Khodov, M. G. Kiselev, V. V. Klochkov, S. V. Efimov – or Life is about compromises, J. Magn. Reson. 2016, 266, 69-72.
51 C. M. Thiele, A. S. Ulrich, Light flips a membrane-embedded helix, Science 2016, 352, 520. [Full Text][PDF Reprint]
52 M. R. M. Koos, G. Kummerlöwe, L. Kaltschnee, C. M. Thiele, B. Luy, CLIP-COSY: A Clean Inphase Experiment for Rapid Acquisition of COSY-type Correlations, Angew. Chem. 2016, 128, 7785-7789, Angew. Chem. Int. Ed. 2016, 55, 7655-7659.
53 L. Kaltschnee, K. Knoll, V. Schmidts, R. W. Adams, M. Nilsson, G. A. Morris, C. M. Thiele, Extraction of Distance Restraints from Pure Shift NOE experiments, J. Magn. Reson. 2016, 271, 99-109.
54 I. Timári, L. Kaltschnee, M. H. Raics, F. Roth, N. G. A. Bell, R. W. Adams, M. Nilsson, D. Uhrín, G. A. Morris, C. M. Thiele, K. E. Kövér, Real-time broadband proton-homodecoupled CLIP/CLAP-HSQC for automated measurement of heteronuclear one-bond coupling constants, RSC Adv. 2016, 6, 87848-87855.
55 J. Kind, L. Kaltschnee, M. Leyendecker, C. M. Thiele, Distinction of trans-cis photoisomers with comparable optical properties in multiple-state photochromic systems – Examining a molecule with three azobenzenes via in situ irradiation NMR, Chem. Commun. 2016, 52, 12506-12509.
56 S. Hörner, S. Knauer, C. Uth, M. Jöst, V. Schmidts, H. Frauendorf, C. M. Thiele, O. Avrutina, H. Kolmar, Nanoscale Biodegradable Organic–Inorganic Hybrids for Efficient Cell Penetration and Drug Delivery, Angew. Chem. 2016, 128, 15063-15068, Angew. Chem. Int. Ed. 2016, 55, 14842-14846.
57 E. Procházková, A. Kolmer, J. Ilgen, M. Schwab, L. Kaltschnee, M. Fredersdorf, V. Schmidts, R. C. Wende, P. R. Schreiner, C. M. Thiele, Uncovering Key Structural Features of an Enantioselective Peptide-Catalyzed Acylation Utilizing Advanced NMR Techniques, Angew. Chem. 2016, 128, 15986–15991, Angew. Chem. Int. Ed. 2016, 55, 15754–15759.
58 C. M. Thiele, Book Review, Csaba Szántay Jr. (Ed.): Anthropic awareness: the human aspects of scientific thinking in NMR spectroscopy and mass spectrometry, Anal. Bioanal. Chem. 2017, 409, 867-868. [Full Text]
59 Yu. E. Moskalenko, V. Bagutski, C. M. Thiele, Chemically synthesized and cross-linked PDMS as versatile alignment medium for organic compounds, Chem. Commun. 2017, 53, 95-98. [Inside Front Cover]
60 M. Fredersdorf, M. Kurz, A. Bauer, M.-O. Ebert, C. Rigling, L. Lannes, C. M. Thiele, Conformational analysis of an antibacterial cyclodepsipeptide active against M. tuberculosis by a combined ROE and RDC analysis, Chem. Eur. J. 2017, 24, 5729-5735. [Back Cover]
61 S. Hansmann, V. Schmidts, C. M. Thiele, Synthesis of Poly-γ-S-2-methylbutyl-L-glutamate and Poly-γ-S 2-methylbutyl-D-glutamate and their Use as Enantiodiscriminating Alignment Media in NMR Spectroscopy, Chem. Eur. J. 2017, 23, 9114-9121.
62 M. Leyendecker, N.-C. Meyer, C. M. Thiele, Development of new supramolecular lyotropic liquid crystals and their application as alignment media for organic compounds, Angew. Chem. 2017, 129, 11629-11632, Angew. Chem. Int. Ed. 2017, 56, 11471-11474.
63 M. Schwab, D. Herold, C. M. Thiele, Polyaspartates as Thermoresponsive Enantiodifferentiating Helically Chiral Alignment Media for Anisotropic NMR-Spectroscopy, Chem. Eur. J. 2017, 23, 14576-14584.
64 S. Ortgies, R. Rieger, K. Rode, K. Koszinowski, J. Kind, C. M. Thiele, J. Rehbein, A. Breder, Mechanistic and Synthetic Investigations on the Dual Selenium-π-Acid/Photoredox Catalysis in the Context of the Aerobic Dehydrogenative Lactonization of Alkenoic Acids, ACS Catal. 2017, 7, 7578-7586.
65 J. Ilgen, L. Kaltschnee, C. M. Thiele, A pure shift experiment with increased sensitivity and superior performance for strongly coupled systems, J. Magn. Reson. 2018, 286, 18-29.
66 E. Procházková, L. Čechová, J. Kind, Z. Janeba, C. M. Thiele, M. Dračínský, Photoswitchable intramolecular hydrogen bonds in 5-phenylazopyrimidines revealed by in-situ irradiation NMR spectroscopy, Chem. Eur. J. 2018, 24, 492-498.
67 S. Fräbel, B. Wagner, M. Krischke, V. Schmidts, C. M. Thiele, A. Staniek, H. Warzecha, Engineering of new-to-nature halogenated indigo precursors in plants, Metab. Eng. 2018, 46, 20-27.
68 L. Čechová, J. Kind, M. Dračínský, J. Filo, Z. Janeba, C. M. Thiele, M. Cigáň, E. Procházková, Photoswitching behavior of 5-phenylazopyrimidines: in situ irradiation NMR and optical spectroscopy combined with theoretical methods, J. Org. Chem. 2018, 83, 5986-5998.
69 A.-K. Schönbein, J. Kind, C. M. Thiele, J. J. Michels, Full Quantification of the Light-Mediated Gilch Polymerization, Macromolecules 2018, 51, 4678-4687.
70 J. Ilgen, L. Kaltschnee, C. M. Thiele, perfectBASH: Band-selective homonuclear decoupling in peptides and peptidomimetics, Magn. Reson. Chem. 2018, 56, 918-933.
71 S. Weißheit, M. Kahse, K. Kämpf, A. Tietze, M. Vogel, R. Winter, C. M. Thiele, Elastin-like Peptide in Confinement: FT-IR and NMR T1 Relaxation Data, Z. Phys. Chem. 2018, 232, 1239-1261.
72 M. Schwab, V. Schmidts, C. M. Thiele, Thermoresponsive Alignment Media in NMR spectroscopy: Helix Reversal of a Copolyaspartate at Ambient Temperatures, Chem. Eur. J. 2018, 24, 14373-14377.
73 S. Jeziorowski, C. M. Thiele, Poly‐γ‐p‐biphenylmethyl‐glutamate as Enantiodifferentiating Alignment Medium for NMR‐Spectroscopy with Temperature Tunable Properties, Chem. Eur. J. 2018, 24, 15631-15637.